| 3-溴-4-三氟甲氧基苯酚的合成 |
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| 引用本文： | 陈炳和. 3-溴-4-三氟甲氧基苯酚的合成[J]. 化工进展, 2007, 26(12): 1795-1797 |
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| 作者姓名： | 陈炳和 |
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| 作者单位： | 常州工程职业技术学院,江苏,常州,213164 |
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| 摘 要： | 以邻三氟甲氧基苯胺为原料经硝化、重氮化、还原和水解四步可得纯度≥99%(GC)的产物3-溴-4-三氟甲氧基苯酚,总产率26.2%。产物结构通过MS及1H NMR验证。
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| 关 键 词： | 邻三氟甲氧基苯胺 3-溴-4-三氟甲氧基苯酚 合成 |
| 文章编号： | 1000-6613(2007)12-1795-03 |
| 修稿时间： | 2007-10-21 |
Synthesis of 3-bromo-4-(trifluoromethoxy)phenol |
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| CHEN Binghe. Synthesis of 3-bromo-4-(trifluoromethoxy)phenol[J]. Chemical Industry and Engineering Progress, 2007, 26(12): 1795-1797 |
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| Authors: | CHEN Binghe |
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| Abstract: | 3-bromo-4-(trifluoromethoxy)phenol was synthesized from 2-(trifluoromethoxy)aniline by nitration to give 2-trifluoromethoxy-5-nitroaniline,which subjected to sandmeyer reaction,reduction and hydrolytic action with an overall yield of 26.2% and purity of 99%.The structure of the product was confirmed by MS and 1H NMR. |
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| Keywords: | 3-bromo-4-(trifluoromethoxy)phenol 2-(trifluoromethoxy)aniline synthesis |
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