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沉淀分离-络合滴定法测量硫化钠含量
引用本文:吴豫鄂. 沉淀分离-络合滴定法测量硫化钠含量[J]. 武汉化工学院学报, 2006, 28(2): 17-18
作者姓名:吴豫鄂
作者单位:武汉化工学院分析测试中心,湖北武汉430074
摘    要:介绍了ZnS沉淀分离-EDTA络合滴定法测量工业硫化钠中Na2S含量的原理和方法,并对该方法的准确性和重现性进行了论证.实验结果表明:该方法具有良好的重现性,重复实验的相对标准偏差为0.55%;该方法具有较高的准确性,与碘量法(国标)相比结果相差0.11%,一致性达到99.5%.

关 键 词:硫化钠 分析方法 重现性 准确性
文章编号:1004-4736(2006)02-0017-02
收稿时间:2005-04-27
修稿时间:2005-04-27

Determination content of Na2S with the use of precipitation separation - complexmetric titration
WU Yu - e. Determination content of Na2S with the use of precipitation separation - complexmetric titration[J]. Journal of Wuhan Institute of Chemical Technology, 2006, 28(2): 17-18
Authors:WU Yu - e
Affiliation:Center of Analysis and Test, Wuhan institute of Chemical Technology, Wuhan 430074, China
Abstract:A method for determination content of Na_2S in sodium sulfide was described with the use of ZnS-precipitation separation-EDTA-complexmetric titration,and the repeatability and accuracy on the method were discussed.The results were as followed:good repeatability,good accuracy.Therefore,the method made more way of determination content of Na_2S .
Keywords:sodium sulfide    analysis method    repeatability    accuracy
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