| β-异佛尔酮催化氧化制酮代异佛尔酮 |
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| 引用本文： | 周文勇,叶启亮,黄婕,齐鸣斋. β-异佛尔酮催化氧化制酮代异佛尔酮[J]. 化学世界, 2002, 43(9): 482-483,481 |
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| 作者姓名： | 周文勇 叶启亮 黄婕 齐鸣斋 |
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| 作者单位： | 华东理工大学化学工程系,上海,200037 |
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| 摘 要： | 研究了以 β-异佛尔酮为原料 ,在催化剂存在下 ,用分子氧氧化制备酮代异佛尔酮的合成工艺。考察了催化剂用量、反应温度、反应时间、通氧速率、搅拌速度等因素对酮代异佛尔酮产率的影响。在较佳的实验条件下 ,酮代异佛尔酮的收率达 94%以上
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| 关 键 词： | 异佛尔酮 酮代异佛尔酮 催化氧化 合成 |
| 文章编号： | 0367-6358(2002)09-0482-03 |
Catalytic Oxidation ofβ-Isophorone to Keto-isophorone |
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| ZHOU Wen yong,YE Qi liang,HUANG Jie,QI Ming zhai. Catalytic Oxidation ofβ-Isophorone to Keto-isophorone[J]. Chemical World, 2002, 43(9): 482-483,481 |
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| Authors: | ZHOU Wen yong YE Qi liang HUANG Jie QI Ming zhai |
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| Abstract: | β-isoporone was catalytically oxidized to keto isoporone by molecular oxygen. The effect of catalyst content, reaction temperature, reaction time, oxygen content and agitator velocity on preparation of keto isoporone was investigated. The yield of keto isophorone was over 94% under optimum conditions. |
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| Keywords: | isophorone keto isophorone catalytic oxidation synthesis |
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