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Dielectric properties of spark plasma sintering AlN-W composite ceramics
Authors:Jiangyuan Wang  Xian Jia  Chengchang Jia  Guixia Dong  Yuli Zhang  Lei Jia
Affiliation:WANG Jiangyuana,JIA Xiana,c,JIA Chengchanga,DONG Guixiab,ZHANG Yulia,and JIA Leia a School of Materials Science and Engineering,University of Science and Technology Beijing,Beijing 100083,China b School of Materials Science and Engineering,Hebei United University,Tangshan 063009,China c Journals Publishing Center,China
Abstract:In order to develop AlN composites suitable for high average power electronic tube, AlN-W materials were prepared by spark plasma sintering. The effects of manufacture parameters on dielectric loss tangent and permittivity constant were investigated, which include powder-mixed method, milling time of high-energy ball milling, starting powder particle size, sintering temperature and holding time and adding amount of the conductive second phase. The results showed that AlN-W materials sintered at the temperature of 1700°C holding for 5 min with 10 vol.% W showed the best dielectric loss tangent larger than 0.81 at the frequency 1 kHz-1 MHz. In addition, magnetic stirring mixed powder and lower sintering temperature led to the better properties because of the higher porosity. The samples sintered from the starting AlN powder with smaller particle size also had the better properties.
Keywords:AlN-W ceramic  spark plasma sintering  dielectric properties  powder mixing methods  microstructures  
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