| ZSiO4/Cd(S1-xSex)包裹色料的水热合成 |
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| 引用本文： | 宋晓岚,彭林,丁意,李媚,王顺葵,屈一新,邱冠周.ZSiO4/Cd(S1-xSex)包裹色料的水热合成[J].硅酸盐学报,2009,37(7). |
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| 作者姓名： | 宋晓岚 彭林 丁意 李媚 王顺葵 屈一新 邱冠周 |
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| 作者单位： | 1. 中南大学资源加工与生物工程学院,长沙,410083
2. 北京化工大学化学化工学院,北京,100029 |
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| 基金项目： | 科技部国际科技合作计划，教育部国家大学生创新实验计划 |
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| 摘 要： | 采用水热法成功合成了ZrSiO4/Cd(S1-xSex包裹色料,通过x射线衍射、透射电子显微镜、红外光谱及色度测试研究了合成条件对色料性能的影响.结果表明:当水热反应温度为180℃,保温时间为10h,ZrSiO4/Cd(S1-xSex=2时,色料具有较好的结晶度和色度,粒子细小且均匀,其尺寸分布为20～30nm.
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| 关 键 词： | 硅酸锆/硫硒化镉 包裹色料 水热合成 |
HYDROTHERMAL SYNTHESIS OF ZrSiO4/Cd(S1-xSex) INCLUSION PIGMENT |
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| SONG Xiaolan,PENG Lin,DING Yi,LI Mei,WANG Shunkui,QU Yixing,QIU Guanzhou.HYDROTHERMAL SYNTHESIS OF ZrSiO4/Cd(S1-xSex) INCLUSION PIGMENT[J].Journal of The Chinese Ceramic Society,2009,37(7). |
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| Authors: | SONG Xiaolan PENG Lin DING Yi LI Mei WANG Shunkui QU Yixing QIU Guanzhou |
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| Abstract: | An inclusion pigment of ZrSiO4/Cd(S1-xSex) was synthesized by a hydrothermal method. The effects of the synthesis pa-rameters (such as temperature, duration and molar ratio of ZrSiO4/Cd(S1-xSex)) on the pigment properties were investigated by X-ray diffraction, transmission electron microscopy, infrared spectroscopy and chromaticity. The results show that the products in the particle size range of 20-30mm with good crystallinity/intensc hues and the narrow size distribution can be obtained in a molar ratio of ZrSiO4 to Cd(S1-xSex) of 2 and at a synthesis temperature of 180℃ for 10h. |
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| Keywords: | zircon cadmium sulfo-selenide inclusion pigments hydrothermal synthesis |
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