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Synthesis of N-Substituted (Z)-3-( (2-Benzyl)-4-Ox opent-2-yl) Pyrrole-2,5-Diones (Maleimides)
作者姓名:Isra Salih Ad-Daraji,  Albdulmajeed Salih Hamad Alsamarrai
作者单位:[1]Department of Chemistry, College of Education, University of Samarra, Salahalddin 131333, Iraq; [2]Department of Applied Chemistry, College of Applied Science, University of Samarra, Salahalddin 131333, Iraq
基金项目:Acknowledgments We thank department of chemistry, college of education, university of Samarra, Iraq for funding this project. Also, we thank SDI (Samarra Drug Industry) for providing some instrumental facilities.
摘    要:A series of N-substituted (Z)-3-((2-benzyl)-4-oxopent-2-yl)pyrrole-2,5-diones were synthesized and characterized. The compounds were synthesized from dimethyl-2-((Z)-2-(benzylamino)-4-oxopent-2-en-3-yl) fumarate (9) and dimethyl acetylenedi-carboxylate followed by reaction with some amines in refluxing ethanol. The identification of the compounds were based on spectroscopic analysis such as 1R (infrared), UV (ultraviolet), ^1H-NMR (nuclear magnetic resonance) and the microanalysis of the elements (CHN (microanalysis)) data.

关 键 词:马来酰亚胺  N-取代  苄基  吡咯  二酮  羧酸乙酯  富马酸酯  光谱分析
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