Synthesis of N-Substituted (Z)-3-( (2-Benzyl)-4-Ox opent-2-yl) Pyrrole-2,5-Diones (Maleimides) |
| |
作者姓名: | Isra Salih Ad-Daraji, Albdulmajeed Salih Hamad Alsamarrai |
| |
作者单位: | [1]Department of Chemistry, College of Education, University of Samarra, Salahalddin 131333, Iraq; [2]Department of Applied Chemistry, College of Applied Science, University of Samarra, Salahalddin 131333, Iraq |
| |
基金项目: | Acknowledgments We thank department of chemistry, college of education, university of Samarra, Iraq for funding this project. Also, we thank SDI (Samarra Drug Industry) for providing some instrumental facilities. |
| |
摘 要: | A series of N-substituted (Z)-3-((2-benzyl)-4-oxopent-2-yl)pyrrole-2,5-diones were synthesized and characterized. The compounds were synthesized from dimethyl-2-((Z)-2-(benzylamino)-4-oxopent-2-en-3-yl) fumarate (9) and dimethyl acetylenedi-carboxylate followed by reaction with some amines in refluxing ethanol. The identification of the compounds were based on spectroscopic analysis such as 1R (infrared), UV (ultraviolet), ^1H-NMR (nuclear magnetic resonance) and the microanalysis of the elements (CHN (microanalysis)) data.
|
关 键 词: | 马来酰亚胺 N-取代 苄基 吡咯 二酮 羧酸乙酯 富马酸酯 光谱分析 |
本文献已被 维普 等数据库收录! |
|