| 等离子喷涂ZrO2涂层显微结构表征和热导率分析（英文） |
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| 引用本文： | 王墉哲,吴伟,华佳捷,曾毅,郑学斌,周莹,王虎. 等离子喷涂ZrO2涂层显微结构表征和热导率分析（英文）[J]. 无机材料学报, 2012, 0(5): 550-554 |
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| 作者姓名： | 王墉哲 吴伟 华佳捷 曾毅 郑学斌 周莹 王虎 |
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| 作者单位： | 中国科学院 上海硅酸盐研究所,高性能陶瓷和超微结构国家重点实验室;中国科学院 上海硅酸盐研究所,特种无机涂层重点实验室;上海市计量测试研究院 |
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| 基金项目： | Science and Technology Innovation Project of Shanghai Institute of Ceramics(Y17ZC5150G);Research Fund for Nanomaterials of Shanghai(11nm0506900) |
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| 摘 要： | 利用大气等离子喷涂制备了ZrO2涂层,采用扫描电子显微镜结合图像分析的方法对涂层的显微结构特征(总气孔率和大气率)进行了量化表征.同时利用扫描电子显微镜附带X射线扫描成像对涂层内部的微裂纹和大的分隔裂纹的三维分布进行了表征.据此建立了ZrO2涂层显微结构与热导率之间的关系.室温下,涂层N2的热导率较N1的低,因为涂层N2内气孔和微裂纹数较多;在1000℃,由于微裂纹的烧结作用导致热导率增大,所以涂层N2的热导率较N1反而高.高温下,涂层内由微裂纹汇聚而形成的大的分隔裂纹的存在则可以有效地抑制烧结,降低涂层的热导率.
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| 关 键 词： | ZrO2涂层 显微结构 热导率 X射线显微术 |
Microstructure Characterization and Thermal Conductivity Analysis of Plasma Sprayed ZrO2 Coatings |
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| WANG Yong-Zhe,WU Wei,HUA Jia-Jie,ZENG Yi,ZHENG Xue-Bin,ZHOU Ying,WANG Hu. Microstructure Characterization and Thermal Conductivity Analysis of Plasma Sprayed ZrO2 Coatings[J]. Journal of Inorganic Materials, 2012, 0(5): 550-554 |
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| Authors: | WANG Yong-Zhe WU Wei HUA Jia-Jie ZENG Yi ZHENG Xue-Bin ZHOU Ying WANG Hu |
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| Affiliation: | 1. The State Key Lab of High Performance Ceramics and Superfine Microstructure, Shanghai Institute of Ceramics, Chinese Academy of Sciences, Shanghai 200050, China; 2. Key Laboratory of Inorganic Coating Materials, Shanghai Institute of Ceramics, Chinese Academy of Sciences, Shanghai 200050, China; 3. Shanghai Institute of Measurement and Testing Technology, Shanghai 201203, China) |
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| Abstract: | Yttria stabilized zirconia coatings were deposited using two different sets of parameters (N1, N2 coating). The microstructure features, such as total porosity and large porosity, were quantified by means of scanning electron microscope and image analysis. The three-dimensional distribution of microcracks and segmentation cracks was successfully revealed by the X-ray microscopy in the scanning electron microscope with three-dimensional microtomography capability. So the relationship between microstructure and thermal conductivity was found. At room temperature, thermal conductivity of N2 was lower than that of N1 due to larger pores and microcracks. At 1000℃ thermal conductivity of N1 was lower for the sintering of microcracks. The segmentation cracks formed by the propagation of microcracks could effectively reduce the thermal conductivity at high temperature. |
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| Keywords: | ZrO 2 coatings microstructure thermal conductivity X-ray microscopy |
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