| 3-溴-4，5-二羟基苯甲基乙醚的合成 |
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| 引用本文： | 王宗兴,张立新. 3-溴-4，5-二羟基苯甲基乙醚的合成[J]. 化学工程师, 2009, 23(8): 1-3 |
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| 作者姓名： | 王宗兴 张立新 |
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| 作者单位： | 青岛大学,化学化工与环境学院,山东,青岛,266071 |
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| 基金项目： | "863"重点课题资助项目，"863"专题课题资助项目 |
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| 摘 要： | 以香兰素为原料，经溴代、去甲基化、还原、醚化，首次合成了具有生物活性的溴酚类天然产物——3-溴4，5-二羟基苯甲基乙醚，总收率为60％。其结构经IR、1HNMR和元素分析确认。
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| 关 键 词： | 香兰素 3-溴-4,5-二羟基苯甲基乙醚 合成 |
Synthesis of 3-bromo-4,5-dihydroxybenzyl ethyl ether |
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| WANG Zong-xing,ZHANG Li-xin. Synthesis of 3-bromo-4,5-dihydroxybenzyl ethyl ether[J]. Chemical Engineer, 2009, 23(8): 1-3 |
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| Authors: | WANG Zong-xing ZHANG Li-xin |
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| Affiliation: | College of Chemistry;Chemical Engineering and Environment;Qingdao University;Qingdao 266071;China |
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| Abstract: | 3-bromo-4,5-dihydroxybenzyl ethyl ether,which was a natural bromophenol that has potential bioactiveties,was synthesized for the first time by the procedure of using vanillin as a beginning material through bromination,demethylation,reduction and etherification.The total yield was 60%.The structure was confirmed by 1H NMR,IR and elemental analysis. |
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| Keywords: | vanillin 3-bromo-4 5-dihydroxybenzyl ethyl ether synthesis |
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