| 以离子液体为模板剂合成MCM-41介孔分子筛 |
| |
| 引用本文： | 喻娟,徐军,韩丽,卫冬燕,陈宜俍. 以离子液体为模板剂合成MCM-41介孔分子筛[J]. 天津化工, 2010, 24(5): 24-26. DOI: 10.3969/j.issn.1008-1267.2010.05.008 |
| |
| 作者姓名： | 喻娟 徐军 韩丽 卫冬燕 陈宜俍 |
| |
| 作者单位： | 郑州大学化工与能源学院,河南,郑州,450001 |
| |
| 摘 要： | 以离子液体1-十六烷基-3-甲基溴代咪唑为模板剂,合成介孔分子筛MCM-41。考察了不同硅源[、C16mim]Br/SiO2配比、pH值、晶化时间等条件对合成MCM-41的影响。采用XRD和低温氮吸附对产物进行表征,结果表明该方法合成的样品具有较大比表面积和规整介孔孔道结构。
|
| 关 键 词： | 离子液体 介孔分子筛 MCM-41 合成 |
Synthesis of mesoporous molecular sieves MCM-41 using Ionic liquid as template |
| |
| YU Juan,XU Jun,HAN Li,WEI Dong-yan,CHEN Yi-liang. Synthesis of mesoporous molecular sieves MCM-41 using Ionic liquid as template[J]. Tianjin Chemical Industry, 2010, 24(5): 24-26. DOI: 10.3969/j.issn.1008-1267.2010.05.008 |
| |
| Authors: | YU Juan XU Jun HAN Li WEI Dong-yan CHEN Yi-liang |
| |
| Affiliation: | liang(School of Chemical Engineering and Energy,Zhengzhou University,Zhengzhou 450001,China) |
| |
| Abstract: | Mesoporous molecular sieves MCM-41 has been synthesized using 1-hexadecane-3-methyl-imidazolium bromide as a template.The effects of different Si sources,[C16 mim]Br/SiO2,pH and crystallization time on synthesis of MCM-41.The structure of MCM-41 was characterized by X-ray diffraction and N2 adsorption-desorption.Results show that these mesoporous materials possess higher surface area. |
| |
| Keywords: | MCM-41 |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
