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Biomimetic synthesis of spherical nano-hydroxyapatite in the presence of polyethylene glycol
Authors:Chaofan Qiu  Xiufeng XiaoRongfang Liu
Affiliation:College of Chemistry and Materials Science, Fujian Normal University, Fuzhou 350007, PR China
Abstract:Spherical nano-hydroxyapatite (nano-HA) was synthesized successfully by a biomimetic method using Ca(NO3)2·4H2O and (NH4)3PO4·3H2O as reagents in the presence of polyethylene glycol (PEG). The crystalline phase, microstructure, chemical composition, and morphology of the obtained samples were characterized by X-ray powder diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), and transmission electron microscopy (TEM). The results show that spherical nano-HA with diameter of 30–50 nm can be synthesized in the presence of a certain concentration (2–6%) of PEG. The crystallinity of HA powder synthesized in the presence of PEG was higher than that synthesized in the absence of PEG, but the crystallinity of HA reduced with increasing the concentration of PEG. The electrical conductivity (EC) of the solution revealed that PEG reduced the transfer rate of Ca2+ in the process of HA crystallization, indicating the interaction between PEG and HA. The possible mechanism of formation spherical nano-HA was discussed.
Keywords:Polyethylene glycol   Hydroxyapatite   Biomimetic   Spherical
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