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采用溶胶-凝胶法在多孔氧化铝模板上制备立方相WO3纳米线
引用本文:徐宇兴,谭强强,唐子龙,张中太,袁章福. 采用溶胶-凝胶法在多孔氧化铝模板上制备立方相WO3纳米线[J]. 稀有金属材料与工程, 2010, 39(5): 753-755
作者姓名:徐宇兴  谭强强  唐子龙  张中太  袁章福
作者单位:1. 中国科学院过程工程研究所,北京,100190;清华大学,新型陶瓷与精细工艺国家重点实验室,北京,100084
2. 中国科学院过程工程研究所,北京,100190
3. 清华大学,新型陶瓷与精细工艺国家重点实验室,北京,100084
基金项目:National "973" Project,National Natural Science Foundation,Knowledge Innovation Project of Chinese Academy of Sciences,China Postdoctoral Science Foundation,K. C. Wong Education Foundation
摘    要:采用溶胶-凝胶法在纳米孔氧化铝模板上成功制备形貌各异的WO3纳米线.X射线衍射分析表明所制备的WO3纳米线为立方相结构.经扫描电子显微镜观察发现产物多数为菊花状WO3纳米线,其直径约10~80 nm,长约几微米.与空气气氛相比,氩气气氛更有助于WCl6三嵌段共聚物溶胶在多孔氧化铝模板上形成形貌各异的WO3纳米线.

关 键 词:溶胶-凝胶  纳米孔氧化铝模板  WO3纳米线
收稿时间:2009-05-17

Sol-Gel Derived Cubic-Phase WO3 Nanowires on Nano- Porous Alumina Template
Xu Yuxing,Tan Qiangqiang,Tang Zilong,Zhang Zhongtai and Yuan Zhangfu. Sol-Gel Derived Cubic-Phase WO3 Nanowires on Nano- Porous Alumina Template[J]. Rare Metal Materials and Engineering, 2010, 39(5): 753-755
Authors:Xu Yuxing  Tan Qiangqiang  Tang Zilong  Zhang Zhongtai  Yuan Zhangfu
Affiliation:Institute of Process Engineering, Chinese Academy of Sciences, Beijing 100190, China;Institute of Process Engineering, Chinese Academy of Sciences, Beijing 100190, China;State Key Lab of New Ceramics and Fine Processing, Tsinghua University, Beijing 100084, China;State Key Lab of New Ceramics and Fine Processing, Tsinghua University, Beijing 100084, China;Institute of Process Engineering, Chinese Academy of Sciences, Beijing 100190, China
Abstract:WO3 nanowires with various morphologies were prepared on nanoporous alumina template by a simple sol-gel method. X-ray diffraction analysis reveals that the obtained materials are cubic WO3. Scanning electron microscopy shows that the products contain chrysanthemum-shaped WO3 nanowires. The diameter of WO3 nanowires is about 10-80 nm and their length is up to several micrometers. Argon gas atmosphere is more favorable for WCl6-triblock copolymer sol to form WO3 nanowires with different morphologies on nanoporous alumina template than air atmosphere.
Keywords:sol-gel  nanoporous alumina template  WO3 nanowires
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