高速液相色谱法测定2,4-二氨基甲酸乙酯甲苯 |
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引用本文: | 张明道. 高速液相色谱法测定2,4-二氨基甲酸乙酯甲苯[J]. 石油化工, 1986, 0(6) |
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作者姓名: | 张明道 |
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作者单位: | 上海石油化工研究所 |
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摘 要: | 采用高效液相色潜法对2,4-二氨基甲酸乙酯甲苯进行了定量分析。方法选用YWG-苯键合相(10μm)为固定相,甲醇/水为流动相的反相色谱层析系统。本法的相对标准偏差小于1%,回收率为98—102%。
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Determination of Diethyl Toluene-2,4-dicarbamate by High Speed Liquid Chromatography |
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Abstract: | This paper describes a method for the quantitative determination of diethyl toluene-2,4-dicarbamate by HSLC. Phenyl chemically bonded silica(YWG, 10μm) was adopted as the stationary phase, and methanol/water as the mobil phase of the reversed-phase chromatographic system. The relative standard deviation of the method is less than 1%, and the recovery is between 98% to 102%. |
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