| 仲氨改性剂制备低黄变氨基硅油的研究 |
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| 引用本文： | 余晓红,郑绍成,汪小奥,王钰斐. 仲氨改性剂制备低黄变氨基硅油的研究[J]. 辽宁化工, 2011, 40(4): 328-329,348 |
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| 作者姓名： | 余晓红 郑绍成 汪小奥 王钰斐 |
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| 作者单位： | 1. 浙江师范大学行知学院,浙江金华,321004
2. 浙江师范大学化学与生命科学学院,浙江金华,321004 |
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| 基金项目： | 浙江师范大学实验室开放项目 |
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| 摘 要： | 以仲氨改性剂γ-环己基甲基二甲氧基硅烷（氨基硅烷偶联剂）和八甲基环四硅氧烷（D4）为原料,在氢氧化钾（KOH）催化下,制备了低黄变的氨基硅油。较佳合成条件为：氨基偶联剂用量为4.0%,反应时间为4.5 h,反应温度120℃,催化剂用量为0.10%,制得氨基硅油,将其用于纯棉布后整理,能赋予织物较好的柔软性、平滑性、蓬松性、低黄变性以及亲水性。
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| 关 键 词： | 氨基硅油 低黄变 柔软性 偶联剂 |
Preparation of Low-yellowing Amino Silicone Oil With Amino Silane Coupling Agent |
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| YV Xiao-hong,ZHENG Shao-cheng,WANG Xiao-ao,WANG Yv-fei. Preparation of Low-yellowing Amino Silicone Oil With Amino Silane Coupling Agent[J]. Liaoning Chemical Industry, 2011, 40(4): 328-329,348 |
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| Authors: | YV Xiao-hong ZHENG Shao-cheng WANG Xiao-ao WANG Yv-fei |
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| Affiliation: | YV Xiao-hong 1,ZHENG Shao-cheng 2,WANG Xiao-ao2,WANG Yv-fei2(1.Xingzhi College,Zhejiang Normal University,Zhejiang Jinhua 321004,China,2.College of Chemistry and life sciences,China) |
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| Abstract: | Using cyclohexyl methyl dimethoxy silane（amino silane coupling agent） and octamethylcy-clotetrasiloxane（D4） as raw materials,potassium hydroxide（KOH） as the catalyst,low-yellowing amino silicone oil was prepared.The best synthetic conditions were determined as follows： p-coupling agent dosage 4.0%,reaction time 4.5 h,reaction temperature 120 ℃,catalyst dosage 0.10%.The amino silicone oil prepared under above conditions has good application effect in finishing of pure cotton. |
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| Keywords: | Amino silicone oil Low yellowing Softness Coupling agent |
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