| 微波法合成树枝状纳米硫化锑 |
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| 引用本文： | 叶明富,孔祥荣,潘正凯,伊廷锋,诸荣孙,任世彪,雷智平.微波法合成树枝状纳米硫化锑[J].安徽工业大学学报,2012(4):338-341. |
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| 作者姓名： | 叶明富 孔祥荣 潘正凯 伊廷锋 诸荣孙 任世彪 雷智平 |
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| 作者单位： | 安徽工业大学化学与化工学院;北京建筑材料科学研究总院有限公司 |
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| 基金项目： | 国家自然科学基金项目(91023039);安徽工业大学SRTP项目(2011016);北京市科技新星计划项目(2011028);安徽工业大学优秀创新团队(TD201202) |
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| 摘 要： | 以氯化锑、硫脲为原料，采用微波法合成树枝状硫化锑纳米材料。用X射线粉末衍射（XRD）、扫描电子显微镜（SEM）和X射线能谱（EDS）等对Sb2S3晶体的物相及形貌进行分析表征。结果表明制备出的是正交相Sb2S3，长度可达数十微米。并给出树枝状硫化锑纳米材料的可能的形成机理。
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| 关 键 词： | 硫化锑 微波合成 纳米材料 |
Microwave-assisted Synthesis of Branch-like Sb2S3 Nanomaterials |
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| YE Ming-fu,KONG Xiang-rong,PAN Zheng-kai,YI Ting-feng,ZHU Rong-sun,REN Shi-biao,LEI Zhi-ping.Microwave-assisted Synthesis of Branch-like Sb2S3 Nanomaterials[J].Journal of Anhui University of Technology,2012(4):338-341. |
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| Authors: | YE Ming-fu KONG Xiang-rong PAN Zheng-kai YI Ting-feng ZHU Rong-sun REN Shi-biao LEI Zhi-ping |
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| Affiliation: | 1(1.School of Chemistry and Chemical Engineering,Anhui University of Technology,Ma’anshan 243002,China;2.Beijing Building Materials Academy Co.Ltd.Beijing 10004,China) |
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| Abstract: | Nano-sized branch-like antimony sulfide(Sb2S3) was synthesised at large-scale by microwave heating method and using SbCl3 and CS(NH2)2 as raw materials.The as-prepared Sb2S3 nanomaterials were characterized via X-ray diffraction(XRD),scanning electron microscopy(SEM),energy dispersive X-ray spectrometer(EDS).Results show that the prepared product is the orthogonal Sb2S3 csystal phase with length at tens of micrometers.The possible growth mechanism of the Sb2S3nanomaterials was also provided. |
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| Keywords: | antimony sulfide(Sb2S3) microwave synthesis nanomaterials |
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