Synthesis of metal nitrides and carbide powders by a spark discharge method in liquid media |
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Authors: | T. Sato K. Usuki A. Okuwaki Y. Goto |
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Affiliation: | (1) Department of Molecular Chemistry and Engineering, Faculty of Engineering, Tohoku University, 980 Sendai, Japan;(2) Department of Electrical Engineering, Faculty of Engineering, Tohoku University, 980 Sendai, Japan |
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Abstract: | Metal nitrides and carbides powders were synthesized by the spark discharge method in liquid ammonia at 100 °C and 11 kV of the spark discharge voltage and in n-heptane at 25 °C and 7.5 kV using the pellets of aluminum, titanium, iron and chromium as the starting material. The main products were AlN, TiN0.51, -Fe, -Cr2N in liquid ammonia, and Al4C3, TiC, -Fe, Fe2C and Cr7C3 in n-heptane. The agglomerated particle size decreased with increasing melting point of the metal used as the starting material. |
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