| 5,5＇-亚甲基二水杨酰基二水杨酰肼的合成及表征 |
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| 引用本文： | 韦汉昌,何建华,韦群兰.5,5＇-亚甲基二水杨酰基二水杨酰肼的合成及表征[J].广西化工,2012(5):1-2,44. |
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| 作者姓名： | 韦汉昌 何建华 韦群兰 |
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| 作者单位： | [1]广西师范大学,广西桂林541004 [2]南宁地区教育学院,广西南宁530001 |
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| 基金项目： | 广西自然科学基金项目（No.2010GXNSFD013018） |
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| 摘 要： | 以水杨酸为底物合成一种新的对称双酰肼化合物5,5＇-二水杨酰基二水杨酰肼,经红外光谱分析、元素分析及质谱分析,最终的反应产物为标题化合物,纯度为98.2%,产率为75.1%。
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| 关 键 词： | 5 5＇-亚甲基二水杨酰基二水杨酰肼 合成 表征 |
Synthesis and Characterization of N,N＇-（5,5＇-Methylenedisalicylryl）-disalicylhydrazide |
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| WEI Han-chang,HE Jian-hua,WEI Qun-lan.Synthesis and Characterization of N,N＇-（5,5＇-Methylenedisalicylryl）-disalicylhydrazide[J].Guangxi Chemical Industry,2012(5):1-2,44. |
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| Authors: | WEI Han-chang HE Jian-hua WEI Qun-lan |
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| Affiliation: | 1.Guangxi Normal University,Guilin 541004,China;2.Nanning Prefecture Education College,Nanning 530001,China) |
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| Abstract: | Base on salicylic acid,a novel symmetrical dihydrazide,N,N＇-（5,5＇-Methylenedisalicylryl）-disalicylhydrazide,was synthesized and characterized by element analysis,mass spectrometric analysis and IR analysis.The result showed that the final product was the target compound in a high purity of 98.2%,and the yield was 71.3%. |
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| Keywords: | N N＇-（5 5＇-Methylenedisalicylryl）-disalicylhydrazide synthesis structure characterization |
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