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基于流变学的橡胶粉与基质沥青配伍性试验
引用本文:胡松山,谭华,覃润浦,张玉贞.基于流变学的橡胶粉与基质沥青配伍性试验[J].复合材料学报,2018,35(12):3487-3499.
作者姓名:胡松山  谭华  覃润浦  张玉贞
作者单位:1. 广西交通科学研究院有限公司, 南宁 530007; 2. 广西道路结构与材料重点实验室, 南宁 530007; 3. 高等级公路建设与养护技术、材料及装备交通运输行业研发中心, 南宁 530007; 4. 中国石油大学(华东) 化学工程学院, 青岛 266580
摘    要:基于流变学理论研究橡胶粉与不同来源基质沥青的配伍性,采用动态剪切流变仪(DSR)分别对不同基质沥青加工而成的橡胶沥青进行应变扫描、温度扫描、频率扫描等常规动态剪切流变试验,从相位角、复合模量和车辙因子等指标评价橡胶沥青黏弹特性,定性区分沥青四组分对橡胶沥青黏弹特性的影响,并对橡胶沥青进行滞回环试验,运用灰色关联数学分析方法定量给出沥青四组分对橡胶沥青的残余变形、弹性贮能、耗散能、弹性比例和复合弹性模量等指标的影响。结果表明:流变学理论是研究橡胶粉改性剂与基质沥青配伍性的有效方法;从能量角度评价沥青四组分对橡胶沥青黏弹特性指标的影响,沥青质对橡胶沥青残余应变影响较大;胶质组分对橡胶沥青弹性贮能和耗散能影响最大,而芳香分影响最小;沥青质组分对橡胶沥青弹性比例参数影响最大;芳香分含量可以提高橡胶沥青复合模量。

关 键 词:流变学理论  沥青四组分  橡胶沥青  配伍性  黏弹特性  
收稿时间:2017-12-11

Compatibility test of rubber powder and matrix asphalt based on rheology
HU Songshan,TAN Hua,QIN Runpu,ZHANG Yuzhen.Compatibility test of rubber powder and matrix asphalt based on rheology[J].Acta Materiae Compositae Sinica,2018,35(12):3487-3499.
Authors:HU Songshan  TAN Hua  QIN Runpu  ZHANG Yuzhen
Affiliation:1. Guangxi Transportation Research and Consulting CO. LTD., Nanning 530007, China; 2. Guangxi Key Laboratory of Road Structure and Materials, Nanning 530007, China; 3. Research and Development Center on Technologies, Materials and Equipment of High Grade Highway Construction and Maintenance Ministry of Transport, Nanning 530007, China; 4. College of Chemical Engineering, China University of Petroleum, Qingdao 266580, China
Abstract:Rubber powder compatibility with different source matrix asphalts was studied based on the rheological theory.Using dynamic shear rheometer, the different matrix asphalts and rubber asphalts were tested by conventional dynamic shear rheological test, such as strain scanning, temperature scanning and frequency scanning.The viscoelastic properties of rubber asphalt were evaluated from the factors such as the phase angle, composite modulus and rutting factors, and the influence of the four components on the rubber asphalt viscoelastic properties was qualitative.Based on the indices such as the residual deformation, elastic energy-storage, elastic ratio and composite elastic modulus, the effects of modifying agent on the modification and viscoelastic properties of rubber asphalt were analyzed using the hysteresis loop back test specimen.The correlation was obtained by using grey correlation mathematical analysis method.The results show that rheological theory is an effective method for studying the compatibility of rubber powder and substrate asphalt.The influence of the four components of asphalt on the viscoelastic properties of rubber asphalt was evaluated from the energy angle, and the effect of asphalt on the residual strain of rubber asphalt is significant; The colloidal components can influence the elastic storage energy and dissipation of rubber asphalt, and the fragrances have the least impact; The asphaltenes have the greatest influence on the rubber asphalt elastic ratio parameters; The aromatic content increases the composite modulus of rubber asphalt.
Keywords:rheology theory  asphalt four components  rubber asphalt  compatibility  viscoelastic properties  
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