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三维Ag/TiO_2纳米网的制备及其光催化性能研究
引用本文:李玥,宋育泽,邵浦华,李红英,梁剑,高风仙. 三维Ag/TiO_2纳米网的制备及其光催化性能研究[J]. 电镀与精饰, 2018, 0(6): 1-5. DOI: 10.3969/j.issn.1001-3849.2018.06.001
作者姓名:李玥  宋育泽  邵浦华  李红英  梁剑  高风仙
作者单位:河南工程学院材料与化学工程学院,河南郑州,450007
基金项目:国家自然科学基金青年基金资助项目(51608175),河南省教育厅科学技术研究重点资助项目(17B610004
摘    要:采用阳极氧化法在钛网上制备了TiO_2纳米管阵列,并利用循环伏安法在纳米管表面沉积Ag,制备出Ag/TiO_2纳米复合材料。采用扫描电子显微镜、X-射线衍射仪、紫外-可见漫反射光谱等方法对复合材料的形貌、结构、光电性能进行了表征,并以2,4-二硝基苯酚为模型化合物考察了沉积Ag对复合材料光催化性能的影响。结果表明,沉积5圈Ag的Ag/TiO_2复合纳米材料光催化性能最佳,在模拟太阳光照射120 min后,2,4-二硝基苯酚可被完全降解。

关 键 词:TiO2纳米管  Ag  阳极氧化法  循环伏安法  光催化  TiO2 nanotube  Ag  anodic oxidation method  cyclic voltammetry  photocatalysis

Fabrication and Photocayalytic Performance of 3D Net Structure Ag/TiO2 Nanotubes
LI Yue,SONG Yuze,SHAO Puhua,LI Hongying,LIANG Jian,GAO Fengxian. Fabrication and Photocayalytic Performance of 3D Net Structure Ag/TiO2 Nanotubes[J]. Plating & Finishing, 2018, 0(6): 1-5. DOI: 10.3969/j.issn.1001-3849.2018.06.001
Authors:LI Yue  SONG Yuze  SHAO Puhua  LI Hongying  LIANG Jian  GAO Fengxian
Abstract:TiO2 nanotubes were prepared on titanium mesh by anodic oxidation,and Ag was deposited on the surface of TiO2 nanotubes by cyclic voltammetry,resulting in the Ag/TiO2 nanotubes composite material.Morphology,structure and photocatalytic properties of the composite materials were characterized by scanning electron microscopy (SEM),X-ray diffraction (XRD) and UV-visible diffuse reflectance spectroscopy (DRS).The influences of Ag on the photocatalytic properties of composites materials were investigated by using 2,4-dinitrophenal as model compound.Results indicated that the Ag/TiO2 composite nanomaterial with 5 coils Ag nanoparticales have the best photocatalytic performance,and the 2,4-dinitrophenal could be completely degraded after exposure to the simulated sunlight for120 min.
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