| 苯磺酸-3-硝基对甲苯酯的合成及晶体结构 |
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| 引用本文： | 谷利军,杨秉勤,李敏,高波,陆振欢. 苯磺酸-3-硝基对甲苯酯的合成及晶体结构[J]. 化学试剂, 2009, 31(7) |
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| 作者姓名： | 谷利军 杨秉勤 李敏 高波 陆振欢 |
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| 作者单位： | 西北大学,化学系,陕西,西安710069 |
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| 摘 要： | 以对甲苯酚为原料,超声波辅助下高收率得到苯磺酸对甲苯酯,经硝化合成了标题化合物,用IR、1HNMR、元素分析对其进行表征,X-射线分析数据表明苯磺酸-3-硝基对甲苯酯属于单斜晶系,P2(1)/n空间群.
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| 关 键 词： | 苯磺酸-3-硝基对甲苯酯 合成 晶体结构 |
Synthesis and crystal structure of phenyl 4-methyl-3-nitro-benzenesulfonate |
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| GU Li-jun,YANG Bing-qin,LI Min,GAO Bo,LU Zhen-huang. Synthesis and crystal structure of phenyl 4-methyl-3-nitro-benzenesulfonate[J]. Chemical Reagents, 2009, 31(7) |
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| Authors: | GU Li-jun YANG Bing-qin LI Min GAO Bo LU Zhen-huang |
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| Affiliation: | Department of Chemistry;Northwest University;Xi'an 710069;China |
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| Abstract: | Phenyl 4-methyl-benzenesulfonate was synthesized from 4-methyl-phenol with high yield under supersonic irradiation.Furthermore,phenyl 4-methyl-3-nitro-benzenesulfonate was synthesized via nitration of 4-methyl-benzenesulfonate and was characterized by IR,1HNMR,and elemental analysis.The crystal structure of phenyl 4-methyl-3-nitro-benzenesulfonate was monoclinic,with a space group of P2(1)/n. |
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| Keywords: | phenyl 4-methyl-3-nitro-benzenesulfonate synthesis crystal structure |
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