| 十二水合硫酸铁铵催化合成乙酸环己酯 |
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| 引用本文： | 李毅群.十二水合硫酸铁铵催化合成乙酸环己酯[J].化学世界,2000,41(11):584-586. |
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| 作者姓名： | 李毅群 |
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| 作者单位： | 暨南大学化学系,广东,广州,510632 |
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| 基金项目： | 广东省博士启动基金,广东省博:974021, |
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| 摘 要： | 以乙酸和环己醇为原料 ,十二水合硫酸铁铵为催化剂催化合成了乙酸环己酯。在优化反应条件下 ,酯收率达 80 .0 %。优化反应条件如下 :醇酸摩尔比为 1 .0∶2 .0 ,催化剂用量为 1 .5～ 2 .5 g,反应温度为 1 0 2～ 1 38°C。实验结果表明催化剂催化性能高 ,反应条件温和 ,方法简单 ,收率优良
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| 关 键 词： | 十二水合硫酸铁铵 催化 合成 乙酸环己酯 |
Synthesis of Cyclohexyl Acetate Catalyzed by Ammonium Ferric Sulfate Dodecahydrate |
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| LI Yi-qun.Synthesis of Cyclohexyl Acetate Catalyzed by Ammonium Ferric Sulfate Dodecahydrate[J].Chemical World,2000,41(11):584-586. |
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| Authors: | LI Yi-qun |
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| Abstract: | Cyclohexyl acetate was synthesized from acetic acid and cyclohexanol catalyzed by ammonium ferric sulfate dodecahydrate. Optimum conditions of esterification were determined with yield of 80.0%. They were as follows: molar ratio of alcohol and acid was 1.0∶2.0, amount of catalyst was 1.5~2.5 g and temperature of reaction was 102~138°C. Experimental results showed high catalytic activity, mild conditions, the method convenient and excellent yield. |
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| Keywords: | ammonium ferric sulfate dodecahydrate catalysis synthesis cycloheaxyl acetate |
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