| 介孔有机-无机杂化材料NH_2-MCM-41的合成与表征 |
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| 引用本文： | 高文秀,王景峰,杨艳艳. 介孔有机-无机杂化材料NH_2-MCM-41的合成与表征[J]. 吉林化工学院学报, 2010, 27(4): 21-23 |
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| 作者姓名： | 高文秀 王景峰 杨艳艳 |
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| 作者单位： | 吉林化工学院,化学与制药工程学院,吉林,吉林,132022 |
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| 摘 要： | 以正硅酸乙酯为硅源,十六烷基三甲基溴化铵为模板剂,合成介孔硅基材料MCM-41.通过有机硅烷偶连法将3-氨丙基三乙氧基硅烷嫁接到介孔材料MCM-41上,得到氨基官能化的介孔材料NH2-MCM-41.利用XRD、FT-IR、N2吸附-脱附和ICP对合成的杂化材料进行表征.
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| 关 键 词： | 杂化材料 MCM-41 化学改性 |
Synthesis and characterization of organic-inorganic hybrid NH2-MCM-41 |
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| GAO Wen-xiu,WANG Jing-feng,YANG Yan-yan. Synthesis and characterization of organic-inorganic hybrid NH2-MCM-41[J]. Journal of Jilin Institute of Chemical Technology, 2010, 27(4): 21-23 |
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| Authors: | GAO Wen-xiu WANG Jing-feng YANG Yan-yan |
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| Affiliation: | (College of Chemical and Pharmaceutical Engineering,Jilin Institute of Chemical Technology,Jilin City 132022,China) |
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| Abstract: | Periodic Mesoporous Organosilicas MCM-41 is synthesized by taking TEOS as silica source and CBTA as template agent.The coupling agent 3-aminopropyl triethoxysilane is introduced into the inorganic mesoporous materials MCM-41,so the amino-functionalized mesoporous material NH2-MCM-41 is obtained.The hybrid material is characterized by means of X-ray diffraction,FT-IR,N2 adsorption-desorption experiments and elemental analysis. |
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| Keywords: | MCM-41 |
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