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过氧化钙的制备研究
引用本文:张顺成. 过氧化钙的制备研究[J]. 河北化工, 2010, 33(9): 19-20,54
作者姓名:张顺成
作者单位:河北理工大学化工与生物技术学院,河北,唐山,063000;唐山市建材产品质量监督检验站,河北,唐山,063000
摘    要:研究了氢氧化钙-氯化铵-双氧水法生产过氧化钙的工艺过程和影响因素。通过单因素实验,得到制备过氧化钙的最佳工艺条件为反应温度26℃、反应时间35 min、稳定剂偏硅酸钠用量14%、双氧水浓度15%、氢氧化钙过量50%、氯化铵用量n(NH4Cl)∶n(Ca(OH)2)=1.5。

关 键 词:过氧化氢  氢氧化钙  氯化铵  过氧化钙  稳定剂

The Research on Preparation of Calcium Peroxide
ZHANG Shun-cheng. The Research on Preparation of Calcium Peroxide[J]. Hebei Chemical Engineering and Industry, 2010, 33(9): 19-20,54
Authors:ZHANG Shun-cheng
Affiliation:ZHANG Shun-cheng,(1.College of Chemistry Engineering and Biological Technology,Hebei Polytechnic University,Tangshan 063000,China;2.The Building Materials,Quality Supervision and Inspection Stations of Tangshan,Tangshan 063000,China)
Abstract:In this paper,calcium peroxide was produced by calcium hydroxide and ammonium chloride with hydrogen perox-ide.The factors of influencing calcium peroxide were investigated.The optimum conditions were determined by the mono-factor experiments.The results showed that reaction time was 35 min,reaction temperature was 26 ℃,stabilizer dosage was 14%,hydrogen peroxide concentration was 9%,excessive amount of calcium hydroxide was 50%,excessive amount of ammonium chloride was n(NH4Cl)∶n(Ca(OH)2)=1.5.
Keywords:hydrogen peroxide  calcium hydroxide  ammonium chloride  calcium peroxide  stabilizer
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