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从富铼渣中回收铼并制备高铼酸铵
引用本文:王俊娥,张焕然,衷水平,陈杭.从富铼渣中回收铼并制备高铼酸铵[J].有色金属(冶炼部分),2017(10):57-60.
作者姓名:王俊娥  张焕然  衷水平  陈杭
作者单位:紫金矿业集团股份有限公司,紫金矿业集团股份有限公司,紫金矿业集团股份有限公司,厦门紫金矿冶技术有限公司
基金项目:福建省中科院STS计划配套项目(2016T3033)
摘    要:研究从富铼渣中回收并制备铼产品的工艺路线,着重考察药剂浓度、相比、时间等对铼萃取—反萃的影响,并探索进行了结晶制备高铼酸铵试验。结果表明,经过压力浸出,铼的浸出率达98%以上;在优化试验条件下,铼萃取率可达99.98%,反萃率达到99%以上,一次结晶所得高铼酸铵纯度为98.7%。

关 键 词:富铼渣  萃取  反萃  高铼酸铵
收稿时间:2017/5/4 0:00:00
修稿时间:2017/5/4 0:00:00

Rhenium Recovery from Rhenium Slag and Preparation of Ammonium Perrhenate
WANG Jun-e,zhanghuanran,zhongshuiping and chenhang.Rhenium Recovery from Rhenium Slag and Preparation of Ammonium Perrhenate[J].Nonferrous Metals(Extractive Metallurgy),2017(10):57-60.
Authors:WANG Jun-e  zhanghuanran  zhongshuiping and chenhang
Affiliation:Zijin Mining Group Company,,,
Abstract:Process to recover rhenium from rhenium-rich slag and prepare rhenium products was studied. Effects of agent concentration, phase ratio, and time on extraction and stripping of rhenium extraction were investigated. Preparation of ammonium perrhenate by crystallization was explored. The results show that rhenium leaching rate during pressure leaching is 98% above. Rhenium extraction rate is 99.98%, and rhenium stripping rate is 99% above under the optimum condition. Purity of ammonium perrhenate is 98.7%.
Keywords:rhenium-rich slag  extraction  stripping  ammonium perrhenate
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