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Some observations on the AOAC method for the analysis of brominated oils
Authors:R. R. Lowry  I. J. Tinsley
Affiliation:(1) Dept. of Agricultural Chemistry and Environmental Health Sciences Center, Oregon State University, 97331 Corvallis, OR, 97331
Abstract:Increased sensitivity and improved reproducibility in the analysis by gas liquid Chromatograph y of brominated oils has been ob-tained by re-esterification following denomination. The variety of reactions that can occur at various temperatures and their effects on the procedure are discussed. In addition to defining optimal pro-cedures, it was established that reagents that are more easily and safely handled than metallic sodium give equivalent results. Technical paper no. 5831, Oregon Agricultural Experiment Station.
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