Some observations on the AOAC method for the analysis of brominated oils |
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Authors: | R. R. Lowry I. J. Tinsley |
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Affiliation: | (1) Dept. of Agricultural Chemistry and Environmental Health Sciences Center, Oregon State University, 97331 Corvallis, OR, 97331 |
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Abstract: | Increased sensitivity and improved reproducibility in the analysis by gas liquid Chromatograph y of brominated oils has been ob-tained by re-esterification following denomination. The variety of reactions that can occur at various temperatures and their effects on the procedure are discussed. In addition to defining optimal pro-cedures, it was established that reagents that are more easily and safely handled than metallic sodium give equivalent results. Technical paper no. 5831, Oregon Agricultural Experiment Station. |
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