Reactor Concept for Contactless Kinetic Measurement in Oscillating Droplets via Raman Spectroscopy |
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Authors: | Torsten Klement Norbert Kockmann Thorsten Rder |
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Affiliation: | Torsten Klement,Norbert Kockmann,Thorsten Röder |
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Abstract: | A millistructured reactor and spectroscopic setup for contactless kinetic measurements in oscillating droplets is presented in this work. The polymerization of acrylic acid serves as a model reaction. Design and construction of the reactor focus on the optical access for Raman measurement, the nearly isothermal behavior, and the preservation of droplets during long‐term reactions with a high increase of viscosity. Another key aspect is the possibility of full automation at a later stage. |
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Keywords: | Droplet reactor Kinetic measurement Long reaction times Polymerization process Raman spectroscopy |
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