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AOS中氯代磺内酯、不饱和磺内酯的测定
引用本文:孔令鸟,夏雄燕,方灵丹,陈青明,余新林. AOS中氯代磺内酯、不饱和磺内酯的测定[J]. 日用化学品科学, 2012, 35(10): 20-23,32
作者姓名:孔令鸟  夏雄燕  方灵丹  陈青明  余新林
作者单位:1. 浙江赞宇科技股份有限公司,浙江杭州,310009
2. 嘉兴赞宇科技有限公司,浙江嘉兴,314201
摘    要:烯烃磺酸盐(AOS)中的氯代磺内酯和不饱和磺内酯被公认为是一种皮肤致敏剂,但国内未见氯代磺内酯和不饱和磺内酯的测定方法。采用气相色谱-质谱法,对AOS中的氯代磺内酯和不饱和磺内酯进行分析,该方法的最低检出限为0.015 mg/kg,具有准确、快速和简单等特点。

关 键 词:氯代磺内酯  不饱和磺内酯  气相色谱-质谱法

Determination of chloro-sultones and unsaturated sultones in alpha olefin sulfonate
KONG Ling-niao,XIA Xiong-yan,FANG Ling-dan,CHEN Qing-ming,YU Xin-lin. Determination of chloro-sultones and unsaturated sultones in alpha olefin sulfonate[J]. Detergent & Cosmetics, 2012, 35(10): 20-23,32
Authors:KONG Ling-niao  XIA Xiong-yan  FANG Ling-dan  CHEN Qing-ming  YU Xin-lin
Affiliation:1. Zhejiang Zanyu Technology Co., Ltd., Hangzhou, Zhejiang 310009, China 2. Jiaxing Zanyu Technology Co., Ltd., Jiaxing, Zhejiang 3104201, China)
Abstract:Chloro-sultones and unsaturated sultones in alpha olefin sulfonate have been well-known as skin sensitizers. However, the method to determine chloro-sultones and unsaturated suhones has not been reported domestically. In this paper, chloro-sultones and unsaturated suhones were identified by GC-MS method with the characteristics of accuracy, speediness and simpleness. The detection limit achieves 0.015 mg / kg.
Keywords:chloro-suhones  unsaturated sultones  GC-MS
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