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Apparatus for rapid casting of tubular cellulose acetate reverse osmosis and ultrafiltration membranes
Authors:W.L. Thayer  Lucien Pageau  S. Sourirajan
Affiliation:Division of Chemistry National Research Council of Canada, Ottawa KIA OR9 Canada
Abstract:An improved apparatus is described for making tubular cellulose acetate membranes for reverse osmosis and ultrafiltration applications. The incorporation of an adjustable centering-bob and a sleeve in the design of the casting-bob housing, and the inclusion of an automatically controlled electrical water probe at the bottom of the casting-bob are the novel features of the apparatus. The adjustable centering-bob offers the capability of regulating the passage for the flow of the casting solution during film casting; this capability makes the casting-bob housing useful for a wide range of casting solution viscosities necessary for making both reverse osmosis and ultrafiltration membranes. The sleeve incorporated in the design makes it possible to switch from one tube-casting to the next immediately without any need for the intermediate time consuming operation of cleaning up the casting-bob system. Thus a single casting-bob housing is sufficient for making a plurality of membranes, one after another, with little loss of time between castings. The water probe maintains in the casting tube any desired length of air-zone for the freshly cast membrane. The operation of the apparatus is amenable to a high degree of automation. These features make the apparatus particularly suitable for industrial utilization.
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