Radiance temperatures at 1500 nm of niobium and molybdenum at their melting points by a pulse-heating technique |
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Authors: | E Kaschnitz A Cezairliyan |
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Affiliation: | (1) Metallurgy Division, National Institute of Standards and Technology, 20899 Gaithersburg, Maryland, USA;(2) Österreichisches Giesserei-Institut, Parkstrasse 21, 8700 Leoben, Austria |
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Abstract: | Radiance temperatures at 1500 nm of niobium and molybdenum at their melting points were measured by a pulse-heating technique. The method is based on rapid resistive self-heating of the strip-shaped specimen from room temperature to its melting point in less than I s and measuring the specimen radiance temperature every 0.5 ms with a high-speed infrared pyrometer. Melting of the specimen was manifested by a plateau in the radiance temperature-versus-time function. The melting-point radiance temperature for a given specimen was determined by averaging the measured values along the plateau. A total of 12 to 13 experiments was performed for each metal under investigation. The melting point radiance temperatures for each metal were determined by averaging the results of the individual specimens. The results for radiance temperatures at 1500 nm are as follows: 1983 K for niobium and 2050 K for molybdenum. Based on the estimates of the uncertainties arising from the use of pyrometry and specimen conditions, the combined uncertainty (two standard-deviation level) in the reported values is ± 8 K.Paper presented at the Fourth International Workshop on Subsecond Thermophysics, June 27–29, 1995, Köln, Germany. |
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Keywords: | emissivity (normal spectral) high-speed pyrometry high-temperature reference points melting molybdenum niobium radiance temperature |
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