Synthesis of Pb(Ni1/3Nb2/3)0.72Ti0.28O3 perovskite ceramics by a reaction-sintering process |
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Authors: | Yi-Cheng Liou Jen-Hsien Chen Yi-Chen Huang Chi-Ting Wu Yow-Renn Chen |
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Affiliation: | (1) Department of Electronic Engineering, Kun-Shan University, Tainan Hsien, Taiwan, R.O.C. |
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Abstract: | Pb(Ni1/3Nb2/3)0.72Ti0.28O3 (PNNT) perovskite ceramics produced by a reaction-sintering process were investigated. Without any calcination, the mixture of PbO, Ni(NO3)2, Nb2O5 and TiO2 was pressed and sintered directly into PNNT ceramics. PNNT ceramics of 100% perovskite phase were obtained. For PNNT sintered for 2 h in PbO compensated atmosphere, maximum density reaches a value 8.49 g/cm3 (99.8% of the theoretical value) at 1250∘C. A maximum dielectric constant 20600 occurred around 37∘C at 1 kHz in PNNT sintered at 1250∘C for 2 h. |
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Keywords: | PNN-PT Dielectric Reaction-sintering process |
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