| 微波无溶剂法合成双酚F |
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| 引用本文： | 佟珊玲,胡玲玲,刁凌宇,陈林,余坚,阎雁.微波无溶剂法合成双酚F[J].广东化工,2011,38(3):47-48. |
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| 作者姓名： | 佟珊玲 胡玲玲 刁凌宇 陈林 余坚 阎雁 |
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| 作者单位： | 广东工业大学轻工化工学院,广东,广州,510006 |
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| 基金项目： | 国家自然科学基金，广东省第3批211工程项目 |
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| 摘 要： | 对甲基苯酚和苯酚混合,加入催化剂,混合研磨.在无溶剂微波辐照下,成功地合成了双酚F.完成了产物分析鉴定,优化了反应条件,使双酚F产率达到39%.
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| 关 键 词： | 微波辐照 无溶剂 对甲基苯酚 苯酚 催化 双酚F |
Synthesis of Bisphenol F by Microwave Irradiation under Solvent-free Conditions |
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| Tong Shanling,Hu Lingling,Diao Lingyu,Chen Lin,Yu Jian,Yan Yan.Synthesis of Bisphenol F by Microwave Irradiation under Solvent-free Conditions[J].Guangdong Chemical Industry,2011,38(3):47-48. |
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| Authors: | Tong Shanling Hu Lingling Diao Lingyu Chen Lin Yu Jian Yan Yan |
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| Affiliation: | (College of Light Industry & Chemical Engineering,Guangdong University of Technology, Guangzhou 510006,China) |
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| Abstract: | Phenol and p-methyl phenol were mixed together with a catalyst.After fine grinding,the mixture was irradiated under microwave(600 W) for 5 min’s reaction,and a product,bisphenol F was prepared successfully.The product was characterized and the reaction conditions were optimized.The yield of bisphenol F reached 39% in the microwave irradiation method. |
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| Keywords: | Microwave irradiation solvent-free 4-methyl phenol phenol catalysis bisphenol F |
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