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硫酸镍溶液产品中11种微量元素ICP-OES同时测定
引用本文:张雷,周永生. 硫酸镍溶液产品中11种微量元素ICP-OES同时测定[J]. 广东化工, 2011, 38(3): 129-130,126
作者姓名:张雷  周永生
作者单位:深圳市计量质量检测研究院,广东深圳,518055
摘    要:用ICP-OES法测定硫酸镍溶液产品中的钙、镉、钴、铬、铜、铁、镁、锰、钠、铅、锌11种元素含量,用钇作内标校正大量镍基体的干扰。方法检出限可满足日常分析的需要。加标回收率93.9%~105%;相对标准偏差0.34%~3.21%。方法简便、快速、准确。

关 键 词:ICP-OES  硫酸镍溶液产品  微量元素

Simultaneous Determination of 11 Components in Nickel Sulfate Sioution by ICP-OES
Zhang Lei,Zhou Yongsheng. Simultaneous Determination of 11 Components in Nickel Sulfate Sioution by ICP-OES[J]. Guangdong Chemical Industry, 2011, 38(3): 129-130,126
Authors:Zhang Lei  Zhou Yongsheng
Affiliation:(Shenzhen Measurement Quality Inspection Institute,Shenzhen 518055,China)
Abstract:A method of the determination of 11 components in nickel sulfate by ICP-OES has been presented.The interference effect of matrix was effectively corrected by use of internal standard Y.The method detection limits was determined and met the need of daily analysis.The recovery rates are in the rang of 93.9%~105%,with precision of 0.34%~3.21% RSD.The method is accurate,rapid and simple.
Keywords:ICP-OES
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