| 腰果酚有效成分的定性分析 |
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| 引用本文： | 陈颖怡,谭朝勤.腰果酚有效成分的定性分析[J].广东化工,2009,36(6):169-171,267. |
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| 作者姓名： | 陈颖怡 谭朝勤 |
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| 作者单位： | 广州海关,化验中心,广东,广州,510623 |
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| 摘 要： | 为了分析腰果酚中的有效成分，采用红外光谱仪（IR）对腰果酚进行初步定性；然后采用气相-质谱联用仪（GC／MS）对腰果酚有效成分进行有效分离和准确定性。色谱柱：DB-5柱（30mm×0．25mm×0．25μm）；溶剂：氯仿；柱温：起始温度210℃（保持3．0min），升温速率1℃2／min，最终温度230℃（保持3．0min）。在此条件下，腰果酚中的有效成分可以较好的分离。
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| 关 键 词： | 腰果酚有效成分 红外光谱仪 气相-质谱联用仪 |
Qualitative Analysis of the Active Composition of Cardanol |
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| Chen Yingyi,Tan Zhaoqin.Qualitative Analysis of the Active Composition of Cardanol[J].Guangdong Chemical Industry,2009,36(6):169-171,267. |
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| Authors: | Chen Yingyi Tan Zhaoqin |
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| Affiliation: | Chen Yingyi,Tan Zhaoqin (Laboratory,Guangzhou Customs,Guangzhou 510623,China) |
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| Abstract: | In order to analyze the active composition of cardanol, the preliminary analysis of it was carried out by using infrared spectroscopy （1R）; the active composition of cardanol was separated availably and was analyzed truly by using gas chromatograph-mass spectrometer（GC/MS）. Chromatographic column：DB-5 column（30 min×0.25mm×0.25μm）; solvent：chloroform; column temperature： initial temperature 210℃（keeping 3.0 rain）, the effect of rising emperature rate 1 ℃/min, ： final temperature 230 ℃（keeping 3.0 min）. The active composition ofcardanol were separated completely under this chromatographic conditions. |
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| Keywords: | active composition of cardanol IR GC/MS |
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