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雪松松针挥发油成分分析
引用本文:李保民,魏永生,刘广峰,张利,宗志敏.雪松松针挥发油成分分析[J].化工时刊,2005,19(3):1-3.
作者姓名:李保民  魏永生  刘广峰  张利  宗志敏
作者单位:中国矿业大学化工学院,江苏,徐州,221000;中国矿业大学化工学院,江苏,徐州,221000;中国矿业大学化工学院,江苏,徐州,221000;中国矿业大学化工学院,江苏,徐州,221000;中国矿业大学化工学院,江苏,徐州,221000
摘    要:以无水乙醇、乙酸乙酯、石油醚为溶剂.采用分级萃取的方法分别从新鲜和干枯雪松松针中提取挥发油,利用气相色谱/质谱联用仪(GC-MS)对其化学成分进行分析鉴定。结果表明:新鲜松针中有65种组分,其主要成分是烷烃、烯酸、烯酮、甾醇类,而干枯松针的组分有44种,其主要成分是烷酸、酮类、酯类以及甾醇类物质,其中甾醇类物质的含量比较高。干枯松针中的组分存在形式相对比较稳定。

关 键 词:GC-MS  分级萃取  挥发油  雪松针
修稿时间:2004年10月9日

Composition analysis of cedar
Li Baomin,Wei Yongsheng,Liu Guangfeng,Zhang Li,Zong Zhimin.Composition analysis of cedar[J].Chemical Industry Times,2005,19(3):1-3.
Authors:Li Baomin  Wei Yongsheng  Liu Guangfeng  Zhang Li  Zong Zhimin
Abstract:Volatile oil was extracted from fresh and sear cedar needles by grding extraction with the solvent of anbydrous alcohol?ethyl acetate and petroleum ether.The chemical components was analyzed and identified with gas chromatography/mass spectroleum.There are 65 kinds of compositions in fresh cedar needles where the main components are alkanes?olefine acids?ketene and sterols,while 44 kinds of compositions in sear cedar needles where the main components are alkyl-acids?ketones?esters and sterols.The maximum level in fresh and sear cedar needles was sterols.The compositions are more stable in sear cedar needles than in fresh cedar needles.
Keywords:Gas chromatography/mass spectrometry  grading extraction  volatile oil  cedar needles
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