| 不同Ca／P纳米缺钙羟基磷灰石的微波合成和表征 |
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| 引用本文： | 何立志,冯祖德.不同Ca／P纳米缺钙羟基磷灰石的微波合成和表征[J].广州化工,2009,37(4):74-76. |
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| 作者姓名： | 何立志 冯祖德 |
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| 作者单位： | 1. 湘潭市环境保护监测站,湖南,湘潭411104
2. 厦门大学材料科学与工程学院,固体表面物理化学国家重点实验室,福建厦门,361005 |
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| 基金项目： | 福建省科技重大专项基金 |
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| 摘 要： | 通过微波辐射硝酸钙和磷酸的共沉淀物可以快速合成不同Ca／P比的缺钙羟基磷灰石，利用FT—IR、FT—Raman和XRD对产物进行了表征，EDS测定Ca／P比，TEM观察其形貌。结果表明，通过控制反应条件能得到不同Ca／P比的纳米缺钙羟基磷灰石。
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| 关 键 词： | 缺钙羟基磷灰 Ca/P比 非化学计量比 |
Microwave Synthesis and Characterization of Nano-sized Calcium Deficient Hydroxyapatite with Different Ca/P Ratio |
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| HE Li-zhi,FENG Zu-de.Microwave Synthesis and Characterization of Nano-sized Calcium Deficient Hydroxyapatite with Different Ca/P Ratio[J].GuangZhou Chemical Industry and Technology,2009,37(4):74-76. |
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| Authors: | HE Li-zhi FENG Zu-de |
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| Affiliation: | 1 Xiangtan Environmental Protection Monitoring Station;Hunan Xiangtan 411104;2 Department of Materials Science and Engineering;State Key Laboratory of Physical Chemistry at the Solid Surface;Xiamen University;Fujian Xiamen 361005;China |
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| Abstract: | Rapid synthesis of calcium deficient hydroxyapatite with different Ca/P ratio was done by precipitation using calcium nitrate and phosphoric acid and subsequently subjecting to microwave irradiation. The synthesized CDHA was characterized by FT-IR, FT-Raman, and XRD. Ca/P ratio was determined by EDS. Transmission electron microscopy analysis showed needle like or stick like morphology of CDHA. In all, nanosized CDHA with different Ca/P ratio can be synthesized by controlling reaction condtion. |
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| Keywords: | calcium deficient hydroxyapatite Ca/P ratio non-stoichiometry |
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