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炔丙基氯的制备
引用本文:崔志明,刘安昌. 炔丙基氯的制备[J]. 电镀与精饰, 2001, 23(2): 13-15
作者姓名:崔志明  刘安昌
作者单位:武汉化工学院 科研产业处,
摘    要:炔丙基氯以丙炔醇与三氯化磷为原料,不经处理步骤,采用一步合成炔丙基氯最佳工条件为:在温度15℃以下,在煤油作为油相溶剂及分层剂作用下,反应4h,收率可达到83%,经电镀厂家应用试验,镀层光亮度达到98%,覆盖能力达到98%。

关 键 词:炔丙基氯 电镀 制备 丙炔醇 三氯化磷
文章编号:1001-3849(2001)02-0013-03
修稿时间:2000-09-18

Preparation of Propargyl Chloride
CUI Zhi-ming,LIU An-chang. Preparation of Propargyl Chloride[J]. Plating & Finishing, 2001, 23(2): 13-15
Authors:CUI Zhi-ming  LIU An-chang
Abstract:Propargyl chloride was prepared by reacting propargyl aclohol with phosphorous trichloride in one step. The reacting temperature was below 15℃. Kerosene was used as the solution of oil phase and dispersed phas. The reacting time was as long as four howrs. The yield of the propargyl chloride was ≥83%. Subjeted to application, brightness of the coating and covering power of the bath were all ≥98%.
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