| 气相色谱-负化学离子源质谱法分析大葱中28种农药残留 |
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| 引用本文： | 钱家亮,孔菲. 气相色谱-负化学离子源质谱法分析大葱中28种农药残留[J]. 福建分析测试, 2011, 20(3): 44-48 |
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| 作者姓名： | 钱家亮 孔菲 |
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| 作者单位： | 临沂出入境检验检疫局;临沂市河东区凤凰岭小学; |
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| 摘 要： | 气相色谱-负化学离子化质谱法(CC-NCI-MS)同时分析了大葱中28种农药残留.试样用乙腈提取,PSM/SAX柱净化,采用GC-NCI-MS的选择离子监测方式(SIM)对28种农药残留进行定性与定量分析.28种农药残留的检测限为0.0002-0.05mg/kg.在0.01-0.1 mg/kg添加水平,大葱中农药的的平...
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| 关 键 词： | 负化学离子源 大葱 农药多残留 分析 |
Determination of Multi-Pesticide Residues in Scallion by GC-NCI-MS |
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| Qian Jia-liang,Kong Fei. Determination of Multi-Pesticide Residues in Scallion by GC-NCI-MS[J]. Fujian Anal Ysis & Testing, 2011, 20(3): 44-48 |
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| Authors: | Qian Jia-liang Kong Fei |
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| Affiliation: | Qian Jia-liang,Kong Fei(1.Linyi Exit/Entry Inspection and Quarantine Bureau,Linyi,Shandong276034,China,2.School of Fenghuangling,China) |
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| Abstract: | A method is described for the determination of multi-pesticide residues in scallion by GC-NCI-MS.Scallion samples were extracted with acetonitrile and the extracts were cleaned up by SPE column filled with mix type SAX-PSA,followed by determination with GC-NCI-MS at selected ion monitor mode（SIM）.The detection of the all pesticides were 0.0002～0.05 mg/kg.When the spiked concentrations were 0.01～0.1 mg/kg,all the recoveries of pesticide in scallion were 71.6%～116.8%. |
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| Keywords: | GC-NCI-MS scallion multi-pesticide residues analyze |
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