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A comparative study on the synthesis and properties of suspension and solution precursor plasma sprayed hydroxyapatite coatings
Affiliation:1. Department of Dental Materials and Research Center of Nano-Interface Activation for Biomaterials, and Research Center for Oral Disease Regulation of the Aged, College of Dentistry, Chosun University, Gwangju, Korea;2. Biomechanics and Tissue Engineering Laboratory, Division of Orthodontics, College of Dentistry, The Ohio State University, Columbus, OH, USA;3. Division of Restorative, Prosthetic and Primary Care Dentistry, College of Dentistry, The Ohio State, University, Columbus, OH, USA;1. Mechanical Engineering Department, University Technology PETRONAS, Bandar Seri Iskandar, Perak, Malaysia;2. School of Mechanical Engineering, SRM Institute of Science and Technology, India;3. Gheorghea Asachi Technical University of Iasi, Romania;4. Department of Mechanical Engineering, Bayero University Kano, Nigeria;5. Mechanical Engineering Department, Universitas Pertamina, Kota Jakarta Selatan, Daerah Khusus Ibukota Jakarta 12220, Indonesia;6. Sophisticated Instrument Facility, CRF, Sri Ramachandra Institute of Higher Education and Research, Porur, Chennai 600 116, India;7. Center for Preclinical and Translational Medicine Research, CRF, Sri Ramachandra Institute of Higher Education and Research, Porur, Chennai 600 116, India;8. Central Research Facility, Sri Ramachandra Institute of Higher Education and Research, Porur, Chennai 600 116, India
Abstract:In the present study, hydroxyapatite (HAp) coatings were deposited on Ti-6Al-4V alloy by solution precursor plasma spray (SPPS) and suspension plasma spray (SPS) processes and the properties of the coatings were compared. The feedstock powder for SPS method was prepared by coprecipitation technique and characterized for phase and morphology. The obtained HAp coatings were characterized by X-ray diffractometry, Raman spectroscopy and FT-IR spectroscopy. The biocompatibility of the coatings was evaluated using osteoblast like cells. Both the SPS and SPPS hydroxyapatite coatings exhibited similar crystallinity. Interestingly, the HAp-SPS coating showed marginally higher biocompatibility compared to HAp-SPPS and control samples. The wear and corrosion behavior of these coatings was also studied in Hanks' medium. The hydroxyapatite coating fabricated from SPS technique exhibited better corrosion and wear resistance compared to SPPS coating.
Keywords:Hydroxyapatite  Suspension plasma spraying  Solution precursor plasma spraying  Microstructure  In-vitro
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