| 对叔丁基苯酚催化加氢制备顺式对叔丁基环己醇 |
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| 引用本文： | 熊前政,刘智凌,廖文文,王晓光,刘列琼. 对叔丁基苯酚催化加氢制备顺式对叔丁基环己醇[J]. 精细化工中间体, 2002, 32(2): 25-26 |
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| 作者姓名： | 熊前政 刘智凌 廖文文 王晓光 刘列琼 |
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| 作者单位： | 1. 湖南化工研究院,湖南,长沙,410007
2. 湖北沙隆达集团煤化公司催化剂厂,荆州,434001 |
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| 摘 要： | 采用雷尼镍、Pd/C、Pt/C等为催化剂 ,由对叔丁基酚液相催化加氢合成顺式对叔丁基环己醇。在反应温度 110～ 130℃ ,反应压力 5MPa条件下 ,对叔丁基酚转化率 10 0 % ,对叔丁基环己醇收率 >98% ,顺式对叔丁基环己醇选择性 >75 %
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| 关 键 词： | 对叔丁基苯酚 对叔丁基环己醇 催化 加氢 |
| 文章编号： | 1009-9212(2002)02-0025-02 |
| 修稿时间： | 2001-11-27 |
The Synthesis of cis-4-Tert-butylcyclohexanol from 4-Tert-butylphenol by Catalytic hydrogenation |
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| Xiong Qian Zheng,et al. The Synthesis of cis-4-Tert-butylcyclohexanol from 4-Tert-butylphenol by Catalytic hydrogenation[J]. Fine Chemical Intermediates, 2002, 32(2): 25-26 |
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| Authors: | Xiong Qian Zheng et al |
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| Abstract: | The synthesis of cis 4 tert butylcyclohexanol was studied from 4 tert butylphenol with Ni,Pd/C,Pt/C et al as catalyst by the way of liquid catalytic hydrogenation.The optimun technology Condition were that the reactic temperature was 110～130℃,the reactic pressure was 1～5MPa.The conversion of 4 tert butylphenol was 100%,The yield of 4 tert butylphenolohexanol was over 98%,The selectivity of cis 4 butylcyclohexanol was over 75%. |
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| Keywords: | tert butylcyclohexanol catalysis hydrogenation |
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