| 气相色谱法测定槟榔中甜蜜素含量的不确定度评定 |
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| 引用本文： | 袁 河,陈慧鹏,夏延斌,赵志友,江日初.气相色谱法测定槟榔中甜蜜素含量的不确定度评定[J].食品安全质量检测技术,2019,10(1):215-219. |
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| 作者姓名： | 袁 河 陈慧鹏 夏延斌 赵志友 江日初 |
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| 作者单位： | 湖南省槟榔加工与食用安全工程技术研究中心湖南宾之郎食品科技有限公司;湖南农业大学食品科技学院;湘潭市食品药品监督管理局 |
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| 基金项目： | 湖南省科技创新计划项目(2017TP2028, 2017ZK3138)、长株潭国家自主创新示范区专项(2017SK2430) |
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| 摘 要： | 目的评定气相色谱法测定食用槟榔中环己基氨基磺酸钠(又名甜蜜素)的不确定度评定方法。方法根据气相色谱法定量测定食用槟榔中甜蜜素含量的测定原理,较全面的考虑整个测定过程的不确定度来源,建立结果不确定度评定的数学模型,并探讨其测定结果不确定度。结果在95%的置信区间下,当槟榔中甜蜜素含量为6.19 g/kg时,其扩展不确定度为0.18 g/kg, k=2。结论槟榔中甜蜜素的检测不确定度主要来源为标准曲线的拟合。
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| 关 键 词： | 槟榔 甜蜜素 不确定度 气相色谱法 |
| 收稿时间： | 2018/10/20 0:00:00 |
| 修稿时间： | 2018/12/13 0:00:00 |
Uncertainty evaluation of sodium cyclamate content in Areca catechu L. by gas chromatography |
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| YUAN He,CHEN Hui-Peng,XIA Yan-Bin,ZHAO Zhi-You and JIANG Ri-Chu.Uncertainty evaluation of sodium cyclamate content in Areca catechu L. by gas chromatography[J].Food Safety and Quality Detection Technology,2019,10(1):215-219. |
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| Authors: | YUAN He CHEN Hui-Peng XIA Yan-Bin ZHAO Zhi-You and JIANG Ri-Chu |
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| Affiliation: | Hunan Areca Processing and Edible Safety Engineering Technology Research Center, Hunan Bingzhilang Food Science and Technology Co. Ltd.,Hunan Areca Processing and Edible Safety Engineering Technology Research Center, Hunan Bingzhilang Food Science and Technology Co. Ltd.,Xiangtan Food and Drug Administration,Hunan Areca Processing and Edible Safety Engineering Technology Research Center, Hunan Bingzhilang Food Science and Technology Co. Ltd. and Xiangtan Food and Drug Administration |
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| Abstract: | Objective To evaluate the uncertainty of determination of sodium cyclamate (also known as cyclamate) in edible betelnut by gas chromatography. Methods Based on quantitative determination of sodium cyclamate in edible betelnut by gas chromatography, and more comprehensive consideration of the source of uncertainty throughout the measurement process, a mathematical model for evaluating the uncertainty of results was established and the uncertainty of its measurement results was explored. Results At the 95% confidence interval, when the content of sodium cyclamate in the sample was 6.19 g/kg, its extended uncertainty was 0.18 g/kg (k=2). Conclusion The main source of uncertainty for the detection of cyclamate in betel nut is the fitting of the standard curve. |
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| Keywords: | Areca catechu L sodium cyclamate uncertainty gas chromatography |
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