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鲜、干品红丝线叶挥发油化学成分的GC - MS分析
引用本文:蒋小华,谢运昌,李娟,宁德生.鲜、干品红丝线叶挥发油化学成分的GC - MS分析[J].精细化工,2012,29(4):326-329,351.
作者姓名:蒋小华  谢运昌  李娟  宁德生
作者单位:广西植物功能物质研究与利用重点实验室广西植物研究所,广西桂林,541006
基金项目:广西植物研究所基本科研业务费资助项目( 桂植业09003); 国家科技攻关计划“西部开发” 重大项目(2005BA901A10)
摘    要:采用水蒸气蒸馏法分别得到新鲜和干燥红丝线叶挥发油,并结合GC-MS对所得样品的化学成分进行了分析和鉴定,用气相色谱峰面积归一化法测定各组分的相对质量分数。结果显示,从鲜叶挥发油中鉴定出32种成分,占挥发油总峰面积的98.81%,主要成分是反式植醇(43.29%)、橙花叔醇(7.07%)、石竹烯(4.91%)、亚麻酸甲酯(3.81%)和植酮(3.74%)等;从干叶挥发油中鉴定出42种成分,占挥发油总峰面积的96.23%,反式植醇(33.50%)、橙花叔醇(7.75%)、石竹烯(5.14%)、1-辛烯-3-醇(7.20%)、植酮(4.45%)和樟脑(4.07%)等为主要成分。两者的共有成分有23种,其他化学成分及其相对质量分数存在一定差异。

关 键 词:红丝线  挥发油  化学成分  气相色谱-质谱(GC-MS)  中药现代化技术
收稿时间:2011/12/5 0:00:00
修稿时间:2012/1/10 0:00:00

GC - MS Analysis of Essential Oils from Fresh and Dry leaves of Peristrophe baphica
JIANG Xiao-hu,XIE Yun-Chang,LI Juan and NING De-sheng.GC - MS Analysis of Essential Oils from Fresh and Dry leaves of Peristrophe baphica[J].Fine Chemicals,2012,29(4):326-329,351.
Authors:JIANG Xiao-hu  XIE Yun-Chang  LI Juan and NING De-sheng
Affiliation:Guangxi Key Laboratory of Functional Phytochemicals Research and Utilization, Guangxi Institute of Botany, Chinese Academy of Sciences,Guangxi Key Laboratory of Functional Phytochemicals Research and Utilization, Guangxi Institute of Botany, Chinese Academy of Sciences,Guangxi Key Laboratory of Functional Phytochemicals Research and Utilization, Guangxi Institute of Botany, Chinese Academy of Sciences,Guangxi Key Laboratory of Functional Phytochemicals Research and Utilization, Guangxi Institute of Botany, Chinese Academy of Sciences
Abstract:The essential oils obtained by hydrodistillation from the fresh and dried leaves of Peristrophe baphica,were analyzed by means of gas chromatography-mass spectrometry(GC-MS).A total of 51 volatile components were identified on the basis of their mass spectra characteristics.Thirty-two compounds were identified in the oils of fresh leaves,accounting for 98.81% of the total oils.Among those thirty-two compounds,trans-phytol(43.29%),nerolidol(7.07%),caryophyllene(4.91%),methyl linolenate(3.81%) and phytone(3.74%) were the major ones.Forty-two compounds,representing 96.23% of the total oils,were identified in the dried leaves oils.trans-Phytol(33.50%),nerolidol(7.75%),1-octen-3-ol(7.20%),caryophyllene(5.14%),phytone(4.45%)and camphor(4.07%) were the major compounds.The chemical composition analysis of the essential oils shows that there are only 23 common compounds in the two kinds of essential oils,while the two kinds of oils differ in other chemical constituents and their relative content.
Keywords:Peristrophe baphica  volatile oil  chemical composition  gas chromatography-mass spectrometry(GC-MS)  modernization technology of traditional Chinese medicines
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