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2-[4-(9H-9-咔唑)-苯基]蒽醌的合成与表征
引用本文:何彦波,曹迁永,高希存.2-[4-(9H-9-咔唑)-苯基]蒽醌的合成与表征[J].化学试剂,2010,32(12).
作者姓名:何彦波  曹迁永  高希存
作者单位:南昌大学理学院;
基金项目:国家自然科学基金资助项目
摘    要:以苯酐和咔唑为原料,通过Friedel-Crafts酰基化、浓硫酸催化、Ullman、Suzuki偶联等反应,合成了标题化合物,并对该化合物进行紫外可见吸收和荧光分析。

关 键 词:咔唑  蒽醌  红色荧光  Ullman反应  Suzuki偶联

Synthesis and characterization of 2-(4-(9H-carbazol-9-yl)phenyl)anthracene-9,10-dione
HE Yan-bo,CAO Qian-yong,GAO Xi-cun.Synthesis and characterization of 2-(4-(9H-carbazol-9-yl)phenyl)anthracene-9,10-dione[J].Chemical Reagents,2010,32(12).
Authors:HE Yan-bo  CAO Qian-yong  GAO Xi-cun
Affiliation:HE Yan-bo,CAO Qian-yong,GAO Xi-cun(School of Science,Nanchang University,Nanchang 330031,China)
Abstract:2-(4-(9H-Carbazol-9-yl)phenyl)anthracene-9,10-dione capable of emitting red fluorescent light was synthesized from carbazole and phthalic anhydride through a series of reactions including the Friedel-Crafts reaction,catalysis by concentrated sulfuric acid,and the Ullman and Suzuki coupling reactions.The UV-Vis absorption and fluorescence emission analyses were also used to characterize the title product.
Keywords:carbazole  anthraquinone  red fluorescence  Ullman reaction  Suzuki coupling  
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