| HPLC法测定江西栀子中栀子苷含量研究 |
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| 引用本文： | 廖夫生,侯永春.HPLC法测定江西栀子中栀子苷含量研究[J].广州化工,2011,39(22):68-69,72. |
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| 作者姓名： | 廖夫生 侯永春 |
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| 作者单位： | 江西中医学院药学院,江西南昌,330006 |
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| 基金项目： | 江西省卫生厅科技计划课题(20092053); 江西省教育厅青年科技项目(GJJ10215) |
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| 摘 要： | 用HPLC法测定了江西栀子中栀子苷的含量。色谱柱：Kromasil C18柱（250 mm×416 mm,5μm）;流动相：乙腈-水（15∶85）流速：1.0 mL.min-1;检测波线性长：238 nm;柱温：30℃。结果：栀子苷进样浓度在6.4～32.0μg.mL-1范围内线性关系良好,线性方程为Y=29.802X＋3.75（r=0.9996）,平均回收率为为98.3%。江西不同产地的栀子中栀子苷含量范围在2.9%～3.8%,高于2010版药典规定。
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| 关 键 词： | 高效液相色谱 栀子苷 |
Study of the Assay of Jasminoidin in Gardenia Jasminoides Ellis from Jiangxi by HPLC |
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| LIAO Fu-sheng,HOU Yong-chun.Study of the Assay of Jasminoidin in Gardenia Jasminoides Ellis from Jiangxi by HPLC[J].GuangZhou Chemical Industry and Technology,2011,39(22):68-69,72. |
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| Authors: | LIAO Fu-sheng HOU Yong-chun |
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| Affiliation: | LIAO Fu-sheng,HOU Yong-chun(Jiangxi University of Traditional Chinese Medicine,Jiangxi Nanchang 330006,China) |
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| Abstract: | The determination of jasminoidin in Gardenia jasminoides Ellis from Jiangxi was studied by HPLC.The conditions were Kromasil C18 analyticalcolumn（250 mm×416 mm,5 μm）,mobile phase consisted of acetonitrile-water（15：85）at a flow rate of 1.0 mL·min,detection wavelength was 238 nm and the column temperature was 30 ℃.The method had good liear relationship in the ranges of 6.4～32.0 μg·mL-1 for jasminoidin（r=0.9996）.The average recoveries were 98.3%.The assay of jasminoidin in Gardenia jasminoides Ellis from Jiangxi were 2.9%～3.8%. |
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| Keywords: | HPLC Jasminoides Ellis |
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