| 惰气熔融--热导法测定电解锰中氢 |
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| 引用本文： | 程晓舫,缪琳.惰气熔融--热导法测定电解锰中氢[J].安徽冶金科技职业学院学报,2005,15(1):31-32. |
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| 作者姓名： | 程晓舫 缪琳 |
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| 作者单位： | 马钢股份公司技术中心,安徽,马鞍山,243000;马钢股份公司技术中心,安徽,马鞍山,243000 |
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| 摘 要： | 研究了用Leco公司的RH-404定氢仪分析电解锰中的氢量,采用基准试剂和钢标校准仪器,通过试验找出分析的最佳条件,相对标准偏差为0.76%,氢的加标回收率为95.8%～104.5%,本方法用于电解锰中氢的分析测定,结果令人满意.该方法简单、快速、准确.
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| 关 键 词： | 惰气熔融-热导法 电解锰 氢 |
| 文章编号： | 1672-9994(2005)01-0031-02 |
| 修稿时间： | 2004年10月29日 |
Determination of Hydrogen in Electrolytic Manganese by Inert Gas Fusion- Thermal |
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| CHENG Xiao-fang,Miao Lin.Determination of Hydrogen in Electrolytic Manganese by Inert Gas Fusion- Thermal[J].Journal of Anhui Vocational College of Metallurgy and Technology,2005,15(1):31-32. |
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| Authors: | CHENG Xiao-fang Miao Lin |
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| Affiliation: | CHENG Xiao-fang Miao Lin |
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| Abstract: | In this paper, the determination of hydrogen in electrolytic manganese was studied by RH-404 hydrogen analyzer.The optimal conditions for the analysis have been obtained through calibrating the apparatus by fiducial reagents and standard samples of steel. The relative standard deviation(RSD) were 0.76%. Recoveries between 98.5% to 104.5 %were obtained by standard addition method. The method has been applied the determination of hydrogen in electrolytic manganese with satisfactory results.Analysis by the analyzer showed the spcial features of simple and rapid and accuracy in operatian. |
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| Keywords: | inert gas fusion-thermal conductivity electrolytic manganese hydrogen |
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