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Preparation of sulfur-free exfoliated graphite at a low exfoliation temperature
Affiliation:1. Agricultural Environmental Engineering Center of Sichuan Province, Chengdu, Sichuan 611130, China;2. College of Resources & Environment, Sichuan Agricultural University, Chengdu, Sichuan 611130, China;3. College of Environmental & Resources Sciences, Shanxi University, Taiyuan, Shanxi 030006, China;1. King Abdulaziz University, Faculty of Science, Physics Department, Jeddah, Saudi Arabia;2. Suez Canal University, Faculty of Science, Physics Department, Ismailia, Egypt;3. University of Tabuk, University College, Physics Department, Dhiba, Saudi Arabia
Abstract:Sulfur-free exfoliated graphite at a low exfoliation temperature was prepared from graphite intercalation compounds (GICs) synthesized chemically with different consumption of insertion reagents and oxidants. The effects of their consumption on the synthesis of GICs and of exfoliation temperature on exfoliation volume were studied. The exfoliation volume was 350 ml/g at exfoliation temperature of 200 °C in the best process condition. These results revealed a marked development of the pores in Exfoliated graphite.
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