Acrylic‐based epoxy resin damping systems: Synthesis,characterization, and properties |
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Authors: | Yuan Yang Yun‐Feng Zhao Jian‐Yue Wang Chuan Zhao Liu Tong Xiao‐Yan Liu Mao‐Sheng Zhan |
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Affiliation: | 1. Key Laboratory of Aerospace Materials and Performance (Ministry of Education), School of Materials Science and Engineering, Beihang University, Beijing, China;2. Aerospace Research Institute of Materials & Processing Technology, Beijing, China |
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Abstract: | Acrylate‐based epoxy resin (AE)/low molecular weight polyamine (LPA) composites were developed. The chemical structure, curing behavior, fracture morphology, damping properties, and mechanical properties were evaluated by Fourier transform infrared (FTIR), 1H‐nuclear magnetic resonance (1H‐NMR), gel permeation chromatography (GPC), Differential scanning calorimeter (DSC), scanning electron microscope (SEM), Dynamic mechanical thermal analysis (DMTA), and electro mechanical machine. Transmission electron microscope (TEM) and SEM pictures exhibited nanoscale micro‐phase separation between epoxy and acrylic segmers. DMTA results indicated that the loss factor of cured AE/LPA system could reach 1.84 and temperature range of tan δ > 0.5 was about 84 °C. Tensile strength and elongation at break of the cured AE samples can reach 6.5 MPa and 185%, respectively. © 2016 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2016 , 133, 43654. |
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Keywords: | elastomers manufacturing mechanical properties thermosets viscosity and viscoelasticity |
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