| 磷酸异丁酯类工业样品的NMR分析 |
| |
| 引用本文： | 尚倩,欧阳捷,张巍,邓志威,王丽艳. 磷酸异丁酯类工业样品的NMR分析[J]. 现代仪器, 2007, 13(1): 38-40,37 |
| |
| 作者姓名： | 尚倩 欧阳捷 张巍 邓志威 王丽艳 |
| |
| 作者单位： | 1. 北京师范大学分析测试中心,北京,100875
2. 青岛澳通矿业化工有限公司,山东,266500 |
| |
| 摘 要： | 本工作采用1HNMR和31PNMR结合的方法对工业样品中二硫代磷酸二异丁酯、硫代磷酸二异丁酯、硫代磷酸异丁酯和异丁醇进行表征和定量测量,并对测试的精度和数据的可靠性进行分析。结果表明:所建立的方法可以满足工业生产中质量控制的要求。
|
| 关 键 词： | 核磁共振 定量分析 含磷化合物 |
NMR analysis of industrial samples of thiophosphates |
| |
| Shang Qian,Ouyang Jie,Zhang Wei,Deng Zhiwei,Wang Liyan. NMR analysis of industrial samples of thiophosphates[J]. Modern Instruments, 2007, 13(1): 38-40,37 |
| |
| Authors: | Shang Qian Ouyang Jie Zhang Wei Deng Zhiwei Wang Liyan |
| |
| Abstract: | In this work, industrial samples were analyzed with NMR. With combining application of ^1 H NMR and ^31 P NMR, the components of diisobutyl dithiophosphate, diisobutyl thiophosphate, isobutyl thiophosphate and isobutanol were confirmed,and quantitatively determined. The method was evaluated for the experimental precision and accuracy as well. The results show that this method could satisfy with requirement of the quantitative determination of this products. |
| |
| Keywords: | NMR Quantitative analysis Phosphorus-containing compound |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ |
|
