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Effect of adding methods of metallic phase on microstructure and thermal shock resistance of Ni/(90NiFe2O4-10NiO) cermets
引用本文:赖延清 张勇 田忠良 孙小刚 张刚 李劼. Effect of adding methods of metallic phase on microstructure and thermal shock resistance of Ni/(90NiFe2O4-10NiO) cermets[J]. 中国有色金属学会会刊, 2007, 17(4): 681-685. DOI: 10.1016/S1003-6326(07)60156-3
作者姓名:赖延清 张勇 田忠良 孙小刚 张刚 李劼
作者单位:School of Metallurgical Science and Engineering, Central South University, Changsha 410083, China
基金项目:国家自然科学基金;国家重点基础研究发展计划(973计划);湖南省自然科学基金
摘    要:Ball mixing and electroless plating were respectively used as the adding methods of metallic phase to prepare Ni/(90NiFe2O4-10NiO) cermets for the inert anode in aluminum electrolysis. The microstructure and thermal shock resistance of cermet samples were studied. The results show that, for the samples prepared by ball mixing method, aggregation of metallic phase is found in either the green blocks or sintered samples and the extent of aggregation increases with the increase of metal content. For 6.5Ni/(90NiFe2O4-10NiO) cermets prepared with electroless plating method, the homogeneous and fine metallic particles are found in either the green compacts or sintered samples, but the relative density and thermal shock residual strength decrease by 3% and 28%-58% respectively, compared with samples prepared with ball mixing method.

关 键 词:电镀 金属陶瓷 微观结构 抗热震性 惰性阳极 铝电解
收稿时间:2006-12-04
修稿时间:2006-12-042007-05-14

Effect of adding methods of metallic phase on microstructure and thermal shock resistance of Ni/(90NiFe2O4-10NiO) cermets
LAI Yan-qing,ZHANG Yong,TIAN Zhong-liang,SUN Xiao-gang,ZHANG Gang,LI Jie. Effect of adding methods of metallic phase on microstructure and thermal shock resistance of Ni/(90NiFe2O4-10NiO) cermets[J]. Transactions of Nonferrous Metals Society of China, 2007, 17(4): 681-685. DOI: 10.1016/S1003-6326(07)60156-3
Authors:LAI Yan-qing  ZHANG Yong  TIAN Zhong-liang  SUN Xiao-gang  ZHANG Gang  LI Jie
Affiliation:School of Metallurgical Science and Engineering, Central South University, Changsha 410083, China
Abstract:Ball mixing and electroless plating were respectively used as the adding methods of metallic phase to prepare Ni/(90NiFe2O4-10NiO) cermets for the inert anode in aluminum electrolysis. The microstructure and thermal shock resistance of cermet samples were studied. The results show that, for the samples prepared by ball mixing method, aggregation of metallic phase is found in either the green blocks or sintered samples and the extent of aggregation increases with the increase of metal content. For 6.5Ni/(90NiFe2O4-10NiO) cermets prepared with electroless plating method, the homogeneous and fine metallic particles are found in either the green compacts or sintered samples, but the relative density and thermal shock residual strength decrease by 3% and 28%-58% respectively, compared with samples prepared with ball mixing method.
Keywords:Ni/(90NiFe2O4-10NiO) cermets  microstructure  thermal shock resistance  inert anode  aluminum electrolysis
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