Preparation and characterization of microcapsules containing linseed oil and its use in self-healing coatings |
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Authors: | C. Suryanarayana K. Chowdoji Rao Dhirendra Kumar |
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Affiliation: | 1. Naval Materials Research Laboratory, Shil-Badlapur Road, P.O. Anand Nagar, Additioinal Ambernath (East), Dist. Thane 421506, India;2. Department of Polymer Science and Technology, S.K. University, Anantapur, AP, India |
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Abstract: | Effectiveness of linseed oil filled microcapsules was investigated for healing of cracks generated in paint/coatings. Microcapsules were prepared by in situ polymerization of urea–formaldehyde resin to form shell over linseed oil droplets. Characteristics of these capsules were studied by FTIR, TGA/DSC, scanning electron microscope (SEM) and particle size analyzer. Mechanical stability was determined by stirring microcapsules in different solvents and resin solutions. Cracks in a paint film were successfully healed when linseed oil was released from microcapsules ruptured under simulated mechanical action. Linseed oil healed area was found to prevent corrosion of the substrate. |
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Keywords: | Microencapsulation Self-healing coatings Crack healing Linseed oil |
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