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水质有机污染物GC/MS分析专家系统测定地表水中55种挥发性有机物
引用本文:黄健,王传博,郭春涛,张秀华. 水质有机污染物GC/MS分析专家系统测定地表水中55种挥发性有机物[J]. 现代科学仪器, 2014, 0(2): 112-117
作者姓名:黄健  王传博  郭春涛  张秀华
作者单位:北京普析通用仪器有限责任公司,北京101200
摘    要:使用水质有机污染物GC/MS分析专家系统,按照吹扫捕集/气相色谱-质谱法快速检测地表水中的5 5种挥发性有机物。结果表明,"水质有机污染物GC/MS分析专家系统"快速的实现了55种挥发性有机物的定性定量,其校正曲线相关系数在0.9904-0.9 999之间,样品加标回收率在78.1 9%-128.46%之间,方法检出限在0.03μg/L-1.20μg/L之间,相对标准偏差为2.15%-11.38%。专家系统在水中挥发性有机物检测中具有快速、智能、专用的优势。

关 键 词:水质有机物污染物GC/MS分析专家系统  吹扫捕集/气相色谱-质谱法  地表水  挥发性有机物

Determination of 55 Kinds of Volatile Organic Compounds in Surface Water by GC/MS- Expert-Water System
Huang Jian,Wang Chuanbo,Guo Chuntao,Zhang Xiuhua. Determination of 55 Kinds of Volatile Organic Compounds in Surface Water by GC/MS- Expert-Water System[J]. Modern Scientific Instruments, 2014, 0(2): 112-117
Authors:Huang Jian  Wang Chuanbo  Guo Chuntao  Zhang Xiuhua
Affiliation:(Beijing Purkinje General Instrument Co.,LTD,Beijing 101200)
Abstract:The GC/MS-Expert-Water System was used to detect 55 kinds of volatile organic compounds in surface water, according to the method of purge and trap/gas chromatography-mass spectrometry.The results showed that the GC/MS-Expert-Water Systems quickly realized the qualitative and quantitative analysis of 55 kinds of volatile organic compounds. The correlation coefficients of the calibration curve were between 0.9904-0.9999,and the recoveries were in the range of 78.19%-128.46%.The detection limits were between 0.03gg/L-1.20gg/L,and the relative standard deviation was 2.15% -11.38%. GC/MS-Expert-Water System has the advantage of fast speed, smart ability, it can be applied to the detection of volatile organic compounds in water.
Keywords:GC/MS-Expert-Water System  Purge and trap-gas chromatography/mass spectrometry  Surfacewater  Volatile organic compounds
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