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戊二酸二壬酯的杂多酸催化合成
引用本文:王凤娟. 戊二酸二壬酯的杂多酸催化合成[J]. 精细石油化工进展, 2000, 1(9): 5-7
作者姓名:王凤娟
作者单位:辽阳石油化工高等专科学校,辽阳
摘    要:以杂多酸为催化剂,从二羧酸中分离出戊二酸,再和壬醇反应,合成戊二酸二壬酯。考察了醇酐摩尔比、反应温度、反应时间、催化剂用量等反应条件对酯化反应的影响,确定了合成戊二酸二壬酯的工艺条件,并对目的产物进行了红外光谱测定,按照国家标准,测定了戊二酸二壬酯的一些性能指标。

关 键 词:杂多酸 催化 戊二酸酐 戊二酸二壬酯 合成
修稿时间:2000-07-21

Synthesis of Didecyl Glutarate Catalyzed by Heteropoly Acid
Wang Fengjuan. Synthesis of Didecyl Glutarate Catalyzed by Heteropoly Acid[J]. Advances in Fine Petrochemicals, 2000, 1(9): 5-7
Authors:Wang Fengjuan
Abstract:Didecyl glutarate was synthesized by esterification of n -decanol with glutaric anhydride separated from dicarboxylic acid under the catalysis of heteropoly acid. Effects including molar ratio of alcohol/anhydride,reaction temperature,reaction time,and the amount of catalysts used etc. were ex-amined. The optimum condition was determined. The product was characterized by IR spectrum. Some properties are also outlined.
Keywords:heteropoly acid   esterification   glutaric anhydride   n -decanol   didecyl glutarate
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